燃料与化工 ›› 2017, Vol. 48 ›› Issue (3): 38-41.

• 煤气净化与化学产品加工 • 上一篇    下一篇

9-芴甲醇的合成研究

刘冬杰1  杨峰2  穆春丰2  张春华3   

  1. 1.鞍钢股份有限公司技术中心, 鞍山114009; 2.鞍钢集团化工事业部, 鞍山114000; 3.中冶焦耐工程技术有限公司, 大连116085
  • 出版日期:2017-05-20

Study on synthesis of 9-fluorene methanol

Liu Dongjie1  Yang Feng2  Mu Chunfeng2  Zhang Chunhua3   

  1. 1.Technology Center of Angang Steel Co.,Ltd.,Anshan 114009,China;
     2.Chemical Industrial Division of Ansteel Group Corperation,Anshan 114000,China;
    3.ACRE Coking & Refractory Engineering Consulting Corporation,MCC,Dalian 116085,China
  • Online:2017-05-20

摘要:

利用固体碱为催化剂,采用一步法合成 9-芴甲醇,考察了主要影响因素对产品收率的影响。甲苯和环己烷混合溶剂对粗品提纯能使产品含量达到95%以上,收率达到40%以上。

Abstract:

Solid base was used as catalyst for synthesizing 9-fluorene methanol by “one step method”.The effect of main factors to the yield of product was studied.The mixture solvent of toluene and cyclohexane can improve the purity of the product to 95% and higher,and the yield of the product to 40% and higher.

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