燃料与化工 ›› 2010, Vol. 41 ›› Issue (6): 40-44.

• 煤气净化与化学产品加工 • 上一篇    下一篇

气相色谱-火焰光度法测定苯中微量环丁砜和噻吩

上海宝钢化工有限公司梅山分公司,南京 210039   

  • 出版日期:2010-11-27

Determination of trace sulfolane and thiophene in benzene by gas chromatography flame photometry

Meishan Branch of Shanghai  Baosteel Chemical Co., Ltd, Nanjing 210039, China   

  • Online:2010-11-27

摘要:

建立了气相色谱-火焰光度法测定苯中微量环丁砜和噻吩的方法,对色谱条件进行了优化,定量方法采用外标法。该方法的加标回收率为114%~136%;相对标准偏差(RSD)不大于7%。测定苯样品中微量环丁砜和噻吩具有灵敏度高、重现性好和可靠性高等优点。

Abstract:

The method for the determination of trace sulfolane and thiophene in benzene by gas chromatography flame photometry is established. The chromatography conditions are optimized and the external standard method is adopted for quantitative method. The recovery rates of the method after adding titer range from 114% to 136%. Relative standard deviation is not greater than 7%. The determination of sulfolane and thiophene in benzene sample is characterized by high sensitivity, good reproducibility, high reliability and so on.

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