燃料与化工 ›› 2015, Vol. 46 ›› Issue (5): 52-54.

• 煤气净化与化学产品加工 • 上一篇    下一篇

毛细管气相色谱法分析甲酚异构体

臧娜  王海洋  谷金儒  王守凯   

  1. 中钢集团鞍山热能研究院有限公司, 鞍山114044
  • 出版日期:2015-09-17

Separation and determination of cresol isomers with capillary gas chromatography

Zang Na  Wang Haiyang  Gu Jinru  Wang Shoukai   

  1. Sinosteel Anshan Research Institute of Thermo-Energy Co.,Ltd.,Anshan 114044,China
  • Online:2015-09-17

摘要:

建立一种测定邻甲酚、间甲酚和对甲酚的毛细管气相色谱分析方法。邻甲酚和间甲酚的峰面积与浓度在2~200g/L范围内呈线性关系,相对标准偏差分别为1.84%、1.67%;对甲酚在2~210g/L范围内呈线性关系,相对标准偏差为1.63%,测定回收率均在96.4%~103.8%。

Abstract:

This paper establishes a separation and determination method for o-cresol,m-cresol and p-cresol with capillary gas chromatography.The peak area and concentration of o-cresol and m-cresol have linear relationship in the range of 2~200g/L,and the relative standard deviation is respectively 1.84% and 1.67%; the same of p-cresol has linear relationship in the range of 2~200g/L,and the relative standard deviation is 1.63%.The determined recovery rate of them are all between 96.4%~103.8%.

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